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"The Complete Kinetic Mechanism of Homoisocitrate Dehydrogenanse from Saccharomyces ceresvisiae", Biochemistry, 2007, 46, 890-898. "Reactions of Cysteine Sulfenyl Thiocyanate with Thiols to Give Unsymmetrical Disulfides", Heteroatom Chem, 2007, 18, 467-471. "Molecular Structure and Dynamic Properties of a Sulfonamide Derivative of Glutathione that Is Produced Under Conditions of Oxidative Stress by Hypochlorous Acid", Chemical Research in Toxicology 21(5), 1011-1016, 2008 West, A., "Chemical Mechanism of Homoisocitrate Dehydrogenase from Saccharomyces cerevisiae" Biochemistry, 2008, 47, 4169-4180. “P-31 NMR studies of O-acetylserine sulfhydrylase-B from Salmonella typimurium”. “Phenylethanoid and Lignan Glycosides from Polar Extracts of Lantana: A Genus of Verbenaceous Plants Widely Used in Tradititional Herbal Therapies”. Training will continue throughout the year via remote screen sharing. Mark Morvant and the instrument training will be conducted by the NMR facility manager, Dr. The discussions will be led by an OU Organic Chemistry Faculty member, Dr. the workshop will be divided into parts: effective teaching technique discussions and NMR training. Therefore, four workshops will be hed for the purpose of training and collaboration of the professors.
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It is imperative that both the professors and the students understand how to properly use the instrument. Success of the remote access by the Undergraduate institutions is heavily dependent on the availability and quality of training. Samples will be mailed to the NMR laboratory where a graduate student assistant will make the NMR samples, load the samples into the autosampler and clean the tubes at the conclusion. We will provide additional benefit through on-site training, tours and demonstrations in addition to remote operation and observation of the NMR experiment. Our program will model PNNL in providing teaching and research opportunities to regional undergraduate institutions with the 400 MHz NMR, which is sufficient for our external user base. Undergraduate universities require virtual NMR facilities which are available to them with regards to training, proximity and instrument time. Regional undergraduate institutions have different needs than large research institutions. This program has been successful with regards to bringing high field NMR expertise to other institutions. We will provide resources to these undergraduate institutions much in the same way that the Pacific Northwest National Laboratory (PNNL) operates a virtual NMR facility.
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Several regional undergraduate institutions wish to improve the teaching of their students with NMR experiments however they do not have access to instrumentation. Goal: Provide NMR access to regional undergraduate institutions
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A pdf of this manual can be downloaded from the following link: NMR Facility User Manual(pdf) Supervision of variable temperature experiments will continue until both the NMR facility manager and the student are completely confident of the student's ability to safely carry out these experiments independently.Īll students will be provided a NMR Facility User Manual which details policies and gives step by step instuctions for operation of the instruments. Variable temperature training will be given as needed. The training here represents the most basic and common use of the spectrometers in our department. Unlimited access will be given upon the completion of NMR Test #500-3Īdditional training may be requested on an individual basis. Certification to use the 500 NMR between 8-5 Monday-Friday will be given as NMR Test #500-2 is completed as approved by Dr.
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Training will begin on the 500 upon successful completion of 400 training and Test #500-1. Certification to use the 400 NMR will be given as NMR Test #400-1, and Practical Assignments #400-1 and #400-2 are completed as approved by Dr. Training will begin on the 400 upon successful completion of 300 training. More advanced students and post-docs may gain certification by demonstrating their ability to use the instruments and by completing the assignments.Ĭertification to use the 300 NMR will be given as NMR Test #300-1, Test #300-2 and Practical Assignments #300-1 and #300-2 are completed as approved by Dr. Training sessions will be approximately 45 minutes in duration and will be held as many times as necessary for the student to gain competency. All students will begin training on the 300 NMR.